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Thermal Process Engineering Liquid-Liquid Extraction

Thermal Process Engineering Liquid-Liquid Extraction

Code: TPE0009

Thermal Process Engineering Liquid-Liquid Extraction.

Learning Objectives / Experiments

- transition of a component from a two-component

  liquid mixture into a solvent by extraction
- scale-up from beaker experiment to pilot plant scale
- enrichment of transition component in extract by

  distillation
- evaluation of separation processes via

  concentration

  measurement and mass balances
- influence of different experimental options on

  separation processes

[1] liquid-liquid extraction in counterflow operation with distillation for enrichment of the extract

[2] operation as continuous or discontinuous process using 2 three-way valves
[3] glass extraction column
[4] distillation column and distillation bridge with Liebig condenser

[5] electrical bottom heating via PID controller
[6] water jet pump for reduction of evaporation temperature during distillation
[7] stainless steel tanks for feed, solvent, raffinate, extract and top product (distillation)

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